Practical Liquid Chromatography

1: Liquid Chromatography-The Background.- 1.1. Perspective.- 1.2. Plan of the Book.- 1.3. Chromatography and Its Basic Variants.- 1.3.1. Adsorption Chromatography.- 1.3.2. Ion-Exchange Chromatography.- 1.3.3. Partition Chromatography.- 1.3.4. Exclusion Chromatography.- 1.4. Development Methods in Chromatography.- 1.4.1. Elution.- 1.4.2. Frontal Analysis.- 1.4.3. Displacement.- 1.5. Basic Experimental Arrangements.- 1.5.1. Column Chromatography.- 1.5.2. Layer Chromatography.- 1.6. Measures of the Effectiveness of Chromatographic Separations.- 1.6.1. HETP.- 1.6.2. Resolution.- 1.7. Retention Par.

1: Liquid Chromatography--The Background -- 1.1. Perspective -- 1.2. Plan of the Book -- 1.3. Chromatography and Its Basic Variants -- 1.4. Development Methods in Chromatography -- 1.5. Basic Experimental Arrangements -- 1.6. Measures of the Effectiveness of Chromatographic Separations -- 1.7. Retention Parameters -- References -- Further Reading -- 2: Band Spreading in Chromatography -- 2.1. Introduction -- 2.2. Factors Leading to Band Spreading -- 2.3. The "Random-Walk" Concept -- 2.4. Simple Mathematics of the Random Walk -- 2.5. Molecular Diffusion -- 2.6. Mass Transfer -- 2.7. Eddy Diffusion -- 2.8. Final Expression for Plate Height -- 2.9. Extrabed Contributions to Band Spreading -- 2.10. Columns versus Plates -- 2.11. Summary--Important Practical Consequences of Theory -- References -- Further Reading -- 3: Adsorption Chromatography: Mechanism and Materials -- 3.1. Introduction -- 3.2. Adsorption Isotherms -- 3.3. Nature of Adsorption Forces -- 3.4. Choice of Chromatographie System in LSAC -- 3.5. Variation of Adsorption Coefficient Kº with Solute Structure -- 3.6. Individual Adsorbents -- References -- Further Reading -- 4: Liquid Partition Chromatography--Mechanism and Ma…