Multidimensional NMR methods for the solution state
by Emsley, J. W., (James William) Morris, Gareth A.
The content of this volume has been added to eMagRes (formerly Encyclopedia of Magnetic Resonance) - the .</ The literature of multidimensional NMR began with the publication of three papers in 1975, then nine in 1976 and fifteen in 1977, and now contains many tens of thousands of papers. Any attempt to survey the field must therefore necessarily be very selective, not to say partial. In assembling this handbook, the Editors have sought to provide both the new researcher and the established sci…
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- Full title :Multidimensional NMR methods for the solution state / editors, Gareth A. Morris, James W. Emsley.
Summary
The content of this volume has been added to eMagRes (formerly Encyclopedia of Magnetic Resonance) - the .</ The literature of multidimensional NMR began with the publication of three papers in 1975, then nine in 1976 and fifteen in 1977, and now contains many tens of thousands of papers. Any attempt to survey the field must therefore necessarily be very selective, not to say partial. In assembling this handbook, the Editors have sought to provide both the new researcher and the established scientist with a solid foundation for the understanding of multidimensional NMR, a representative if inevitably limited survey of its applications, an authoritative account of classic techniques such as COSY, NoeSY and TOSCY, and an account of the latest progress in the development of multidimensional techniques.</ This handbook is structured in four parts. The first opens with an historical introduction to, and a brief account of, the practicalities and applications of multidimensional NMR methods, followed by a definitive survey of their conceptual basis and a series of articles setting out the generic principles of methods for acquiring and processing multidimensional NMR data. In the second part, the main families of multidimensional techniques, arranged in approximate order of increasing complexity, are described in detail, from simple J-resolved spectroscopy through to the powerful heteronuclear 3D and 4D methods that now dominate the study of structural biology in solution. The third part offers and illustrative selection from the very wide range of applications of multidimensional NMR methods, including some of the most recent developments in protein NMR. Finally, the fourth part introduces the idea of multidimensional spectra containing non-frequency dimensions, in which properties such as diffusion and relaxation are correlated.</ About EMR Handbooks/ eMagRes Handbooks></ The Encyclopedia of Magnetic Resonance>(up to 2012) and eMagRes>(from 2013 onward) publish a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence of this large number of articles, written by experts in various fields, is enabling the publication of a series of EMR Handbooks/ eMagRes Handbooks>on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of articles from eMagRes>. In consultation with the eMagRes> Editorial Board, the EMR Handbooks/ eMagRes Handbooks> are coherently planned in advance by specially-selected Editors, and new articles are written (together with updates of some already existing articles) to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry.</ Have the content of this Handbook and the complete content of eMagRes>at your fingertips! />Visit: /> />View other eMagRes> publications>
Read More ↓Edition Statements
- Publication Date:©2010
Publication Statements
- Publisher(s):Wiley
- Place of Publication:Chichester, U.K
- Language:eng
- Publication Date:©2010
The Physical Object
- Description:1 online resource (xx, 564 pages) : : illustrations (some color)
Edition Identifiers
- ISBN:9781118589083, 1118589084, 9781118589106, 1118589106
- oclc:ocn827944803
- LC Classification:QC145.4.O6
- Dewey Decimal:543/.66
Table of Contents
Multidimensional NMR Methods for the Solution State; Contents; Contributors; Series Preface; Volume Preface; Part A: Principles; 1 Multidimensional NMR: an Introduction; 1.1 Introduction; 1.2 Historical Background; 1.3 Principles and Practicalities; 1.4 Applications to Liquids; 1.5 Applications to Liquid Crystals; 1.6 Concluding Remarks; References; 2 Multidimensional Spectroscopy: Concepts; 2.1 Introduction; 2.2 Spectroscopy; 2.3 Two-Dimensional and Multidimensional Spectroscopy; 2.4 Coherence Transfer Pathway Selection; 2.5 Building Blocks for Multidimensional NMR Experiments.
2.6 Example of a Multidimensional NMR Experiment: 15N-15N Chemical Shift Correlation for the Sequential Assignment in Proteins2.7 Outlook; References; 3 Ultrafast Multidimensional NMR: Principles and Practice of Single-Scan Methods; 3.1 Introduction; 3.2 The Basis of Gradient-Assisted Single-Scan 2D NMR; 3.3 Setting Up a Single-Scan 2D NMR Acquisition; 3.4 Setting Up Single-Scan 2D NMR's Spatial Encoding; 3.5 Single-Scan 2D NMR: Worked Examples; 3.6 Conclusions and Perspectives; References; 4 Fast Multidimensional NMR by Hadamard Spectroscopy; 4.1 Introduction; 4.2 Hadamard Spectroscopy.
4.3 Higher Dimen…
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