Organic structures from 2D NMR spectra

The derivation of structural information from spectroscopic data is now an integral part of organic chemistry courses at all Universities. Over recent years, a number of powerful two-dimensional NMR techniques (e.g. HSQC, HMBC, TOCSY, COSY and NOESY) have been developed and these have vastly expanded the amount of structural information that can be obtained by NMR spectroscopy. Improvements in NMR instrumentation now mean that 2D NMR spectra are routinely (and sometimes automatically) acquired during the identification and characterisation of organic compounds. Organic Structures from 2D NMR S.

Includes index.

Cover; Title Page; Copyright Page; Contents; Preface; List of Figures; List of Tables; 1 NMR Spectroscopy Basics; 1.1 The Physics of Nuclear Spins; 1.2 Basic NMR Instrumentation and the NMR Experiment; 2 One-Dimensional Pulsed Fourier Transform NMR Spectroscopy; 2.1 The Chemical Shift; 2.2 1H NMR Spectroscopy; 2.2.1 Chemical Shifts in 1H NMR Spectroscopy; 2.2.2 Spin-Spin Coupling in 1H NMR Spectroscopy; 2.2.3 Decoupling in 1H NMR Spectroscopy; 2.2.4 The Nuclear Overhauser Effect in 1H NMR Spectroscopy; 2.3 Carbon-13 NMR Spectroscopy; 2.3.1 Decoupling in 13C NMR Spectroscopy.

2.3.2 Chemical Shifts in 13C NMR Spectroscopy2.4 Fluorine-19 NMR Spectroscopy; 2.5 Phosphorus-31 NMR Spectroscopy; 2.6 Nitrogen-15 NMR Spectroscopy; 3 Two-Dimensional NMR Spectroscopy; 3.1 General Principles; 3.2 Proton-Proton Interactions; 3.2.1 Correlation Spectroscopy -- The COSY Experiment; 3.2.2 Total Correlation Spectroscopy -- The TOCSY Experiment; 3.2.3 Nuclear Overhauser Spectroscopy -- The NOESY Experiment; 3.3 Carbon-Carbon Interactions; 3.3.1 The INADEQUATE Experiment; 3.4 Heteronuclear Correlation Spectroscopy.

3.4.1 Heteronuclear Single Bond Correlation -- The HSQC, HMQC and me-HSQC Experiments…